Tuning 'Metasurface' With Fluid in New Concept for Sensing and Chemistry

A metasurface or metafilm is a two-dimensional version of a metamaterial, popularized recently in technologies with seemingly unnatural properties, such as the illusion of invisibility. Metamaterials have special properties not found in nature, often because of a novel structure. NIST's metasurface is a small piece of composite circuit board studded with metal patches in specific geometries and arrangements to create a structure that can reflect, store, or transmit energy (that is, allow it to pass right through).
As described in a new paper, NIST researchers used purified water to tune the metasurface's resonant frequency -- the specific microwave frequency at which the surface can accumulate or store energy. They also calculated that the metasurface could concentrate electric field strength in localized areas, and thus might be used to heat fluids and promote microwave-assisted chemical or biochemical reactions.
The metasurface's behavior is due to interactions of 18 square copper frame structures, each 10 millimeters on a side (see photo). Computer simulations help design the copper squares to respond to a specific frequency. They are easily excited by microwaves, and each one can store energy in a T-shaped gap in its midsection when the metasurface is in a resonant condition. Fluid channels made of plastic tubing are bonded across the gaps. The sample is placed in a waveguide, which directs the microwaves and acts like a kaleidoscope, with walls that serve as mirrors and create the electrical illusion that the metasurface extends to infinity.

Researchers tested the metasurface properties with and without purified water in the fluid channels. The presence of water shifted the resonant frequency from 3.75 to 3.60 gigahertz. At other frequencies, the metasurface reflects or transmits energy. Researchers also calculated that the metasurface, when in the resonant condition, could concentrate energy in the gaps at least 100 times more than the waveguide alone.